ARCoptix FTIR KIT

The ARCoptix FTIR KIT is a selected set of building blocks that can be seamlessly mounted on the instrument to perform various measurements, offering a compact and highly performant FTIR based platform. The FTIR KIT features a built-in light source, high end ZnSe optics and can host various detectors including a dual-detector version that provides the best of the two worlds: broadband acquisition and high SNR. Each accessory can be ordered individually, which makes the FTIR KIT a versatile tool for laboratories, universities or research institutes.

ATR module

The ATR module consists of a 3 bounce ZnSe ATR crystal designed to measure liquids or suspended solutions. Thanks to the high throughput of this configuration and the high sensitivity of our thermoeletric cooled detectors, the FTIR-KIT-ATR enables all sorts of liquids to be used as buffer, including water !

Diffuse reflectance module

The diffuse reflectance module allows characterizing even low reflective samples over the entire spectral range provided by the selected detector while simultaneously blocking specular reflection. Unlike fibered solutions, this configuration allows collecting high quality spectra with outstanding signa-to-noise ratio in a matter of seconds.

Transmission module

The transmittance module uses focused beams to allow characterizing various optical components (filters, windows etc.) or liquids in a cuvette. High quality transmittance spectra can be effortlessly acquired over a broad spectral range (up to 16 μm) depending on the selected detector.

How does it work?

Permanently aligned interferometer

The heart of the FT-Rocket is dual corner-cube (retro-reflector) interferometer. The two corner-cubes are fixed to a common swinging arm, which rotates to create an optical path difference (with respect to the beam splitter) in the two arms of the interferometer.
This type of design is called a permanently aligned interferometer. This particular arrangement of the interfeormeter is known to be the most robust against vibrations and temperature drifts. It never has to be realigned.
The swinging arm of the interferometer rotates on wear-free flexure system, making this mechanical system extremely robust and durable.

Solid-state reference laser

For measuring the movement of the mirrors, a solid-state reference laser is coupled into the interferometer. Compared to classic HeNe lasers, the solid-state lasers that we use are more compact and have a much longer life-time. They have a very low temperature-induced wavelegnth drift and, when kept at constant temperature with a Peltier element, their wavelength can be stabilized to a few PPM, thus providing a very accurate and reproducible wavelength scale. This is crucial for ensuring a day-to-day and unit-to-unit consistency.

Dual detector option

The performances of the FT-IR spectrometer can be greatly enhanced by integrating a second detector (dual detector configuration) that will boost the signal-to-noise ratio substantially over a selected spectral range (usually 2-6µm).

Model-dependent specifications

Product code	FTIR-KIT-060-4TE-XXX	FTIR-KIT-120-4TE-XXX	FTIR-KIT-160-LN2-XXX
Product code	- ATR (ATR module) - DRA (Diffuse reflectance module) - TRA (Transmittance module)
Beamsplitter material	CaF2	ZnSe
Spectral Range [cm^-1]	5'000 - 1'660	5'000 - 830	5000 - 650
Spectral Range [μm]	2.0-6.0	2.0-12.0	2.0-16.0
Detector Type	MCT (4-TE cooled)		MCT (LN2 cooled)
D* [cm Hz^1/2W^-1]	>1x10E¹¹	>4x10E⁹	>5x10E¹⁰
Signal-to-Noise (4cm^-1 resolution, 1 min scan time)	> 80'000:1	> 40'000:1	> 70'000:1
Built-in light source	20 SiC globar (1550 °K)
Power requirement	40W @12VDC		30W @12VDC

Common specifications

Interferometer type	Permanently aligned, double retro-reflector design
Resolution [cm^-1] (unapodized)	8,4,2
Wavenumber repetability	<10ppm
Scan frequency	>4 Hz @ 4cm^-1
Control laser	Temperature-stabilized solid-state laser @850nm
A/D Converter	24 bit
Operating temperature	10°C-40°C
Communication Interface	USB 2.0 / Ethernet
Software Interface	Windows 10/11 API for controlling the instrument via our DLL
Dimensions	180mm x 160mm x 80mm (excluding LN2 dewar)
Weight	2200 g (excluding LN2 dewar)

Frequently Asked Questions

What is the equivalent wavelength resolution of my FT-IR?

Owing to its operating principle, a FT-IR delivers a spectrum uniformly sampled over a given spectral range in wavenumbers (ν), with units of cm^-1. The wavenumber is simply defined as the inverse of the wavelength (λ). The resolution of an FT-IR is constant in wavenumber (Δν), but varies with wavelength (Δλ) due to the inverse relationship between these two units. The conversion betwen wavenumber resolution and wavelength resolution is Δλ=λ² · Δν and is shown in the graph below:

How to choose the best detector for my application ?

The choice of a detector is a most sensitive one as it contributes to a large extent to the overall quality of your measurement. ARCoptix offers several types and models of detectors, namely extended InGaAs detectors (2 stage thermo-electric cooling), HgCdTe (MCT) detectors with either thermoelectric cooling (4 stages) or liquid nitrogen cooling as well as pyroelectric (DLATGS) detectors. Selection of a given detector is application driven, and depends on the spectral signatures that you are willing to analyze. In order to deliver a faire comparison between various types of photodetectors (or thermal detectors), the most widespread metric is the specific detectivity (labelled D*), which is given in the figure below for all of our available detectors.

Digital Acquisition Acquisition system: AoDAQ

The AoDAQ is a multi-threading, cross-platform and versatile software that simultaneously takes care of:

(1) Handling communication with the FT-IR via USB
(2) Processing raw signals to deliver the spectrum
(3) Running a TCP ethernet server

The AoDAQ can be installed on all sorts of computers, from desktop machines to embedded, low-power single board computers. Thanks to the hosting of a TCP server, the instrument data and parameters can be accessed locally and/or remotely. All communication with the instrument eventually reduces to a set of TCP/IP commands that allow to quickly acquire data, adjust parameters, monitor the instrument status etc. using the programming environment of your choice.

Free GUI basic software

The FTIR Rocket is delivered with a free Windows 7 & Windows 10 compatible graphical user interface (GUI) program.

The free basic software package allows the user to:

Configure hardware measurement parameters (amplifier gain, averaging, ...).
Display real-time spectral measurement results.
Set reference spectra (white, dark) and choose among raw spectra, transmission or reflection mode.
Usual features such as save, open, zoom, rescale...
Some specific features related to Fourier transform spectrometry: choose among spectrum or interferogram averaging, apodization, look and save the interferograms, etc.

Free API & Examples

The FTIR Rocket is also delivered with a free API that allows you to control the spectrometer with custom code via our DLLs. Examples are available for the following languages:

C++
C#
Labview
Matlab

Advanced data processing & analysis software

In collaboration with Labcognition GmbH in Germany we also offer additional Panorama software packages:

Math Add-on module

contains a set of standard manipulation operations used in spectroscopy, like normalization, derivative, baseline correction, peak picking and more. In addition some special operations are available, like multiplicative scatter correction, thickness correction or standard normal variate correction and others.

Quantity Add-on module

is an expert in multivariate data analysis with quantitative methods like PLS and MLR. A convenient and intuitive wizard guides you through all steps of calibration model development. Complex statistical methods become very easy to use even for non-experienced users.

Search Add-on module

is an ideal add-on to archive your spectroscopic data and related information. It includes spectrum and full text search functionality on spectral libraries of various different library formats or directly on data in the file system.

IRAnalyze software package

is a highly sophisticated IR spectrum interpretation tool. Based on an IR spectrum, it provides you with automatic results for IR bands to functional group correlations and their characteristic frequencies. Furthermore, it is a comprehensive electronic dictionary to browse frequiencies for correlated IR bands.

Accessories

Fibered reflection probes

ARCoptix offers three types of optical fiber reflection probes for the near infrared and mid-infrared:

Near-infrared (NIR) reflection probes are made of low-OH fused silica and transmit efficiently between 400 and 2500 nm. (25'000-4'000cm^-1). The bundle consists in 6x 600µm core diameter fibers with one central reading fiber, also with a core diameter of 600µm, held in a ⅛" ferrule.
Indium Fluoride (IFG) reflection probes transmit IR-radiation in the spectral range of 2-5.5μm (1'800 - 5'000cm^-1). The probe consists in 1 500µm core IFG fiber and a one 500µm core IFG fiber for readout that are held in a ¼" ferrule. These probes ideally match the range of our spectrometers using 2-6 µm MCT detectors.
polycrystalline infrared (PIR) reflection probes transmit IR-radiation in the spectral range of 4-18μm.The bundle consists in 6x 400µm core PIR fibers and a single 900µm core PIR fiber for readout that are held in a ¼" ferrule. These fibers ideally match the range of our spectrometers using 2-12 µm MCT detectors.